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5-Methoxyindole

5-Methoxyindole structure

CAS No.: 1006-94-6

Chemical Name:: 5-Methoxyindole

Synonyms: 5-METHOXY-1H-INDOLE;Methoxyindole 99% indol-5-yl methyl ether;5-methoxy-indol;Femedol;NSC 521752;AKOS JY2082918;5-METHOXYINDOLE;methoxy-5indole;5-MethoxyindoleF;Methoxy-5 indole

CBNumber:: CB4223553

Molecular Formula:: C9H9NO

Molecular Weight:: 147.17

MDL Number:: MFCD00005674

MOL File:: 1006-94-6.mol

MSDS File:: SDS

Last updated:2023-05-09 17:25:19

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5-Methoxyindole Properties

Melting point	52-55 °C (lit.)
Boiling point	176-178 °C/17 mmHg (lit.)
Density	1.1135 (rough estimate)
refractive index	1.5310 (estimate)
Flash point	176-178°C/17mm
storage temp.	Keep in dark place,Sealed in dry,Room Temperature
solubility	Chloroform, Methanol
pka	16.70±0.30(Predicted)
form	Crystalline Powder
color	White to light brownish
Water Solubility	insoluble
Sensitive	Light Sensitive
BRN	116722
InChIKey	DWAQDRSOVMLGRQ-UHFFFAOYSA-N
CAS DataBase Reference	1006-94-6(CAS DataBase Reference)
EWG's Food Scores	1
FDA UNII	DQM3AS43PQ
NIST Chemistry Reference	1H-Indole, 5-methoxy-(1006-94-6)

SAFETY

Risk and Safety Statements

Symbol(GHS)

GHS07

Signal word

Warning

Hazard statements

H315-H319-H335

Precautionary statements

P261-P264-P271-P280-P302+P352-P305+P351+P338

Hazard Codes

Risk Statements

36/37/38

Safety Statements

26-36-24/25-37/39

WGK Germany

RTECS

NL9500000

Hazard Note

Irritant

HazardClass

IRRITANT, KEEP COLD, LIGHT SENSITIVE

HS Code

29339900

NFPA 704

	1
2		0

5-Methoxyindole price More Price(31)

Manufacturer	Product number	Product description	CAS number	Packaging	Price	Updated	Buy
Sigma-Aldrich	M14900	5-Methoxyindole 99%	1006-94-6	1g	$25	2023-06-20	Buy
Sigma-Aldrich	M14900	5-Methoxyindole 99%	1006-94-6	5g	$34	2023-06-20	Buy
TCI Chemical	M0731	5-Methoxyindole >99.0%(GC)	1006-94-6	1g	$32	2023-06-20	Buy
TCI Chemical	M0731	5-Methoxyindole >99.0%(GC)	1006-94-6	5g	$55	2023-06-20	Buy
Alfa Aesar	B25290	5-Methoxyindole, 99%	1006-94-6	1g	$41	2023-06-20	Buy

Product number	Packaging	Price	Buy
M14900	1g	$25	Buy
M14900	5g	$34	Buy
M0731	1g	$32	Buy
M0731	5g	$55	Buy
B25290	1g	$41	Buy

5-Methoxyindole Chemical Properties,Uses,Production

Chemical Properties

white to light brownish crystalline powder

Uses

5-Methoxyindole (cas# 1006-94-6) is a compound useful in organic synthesis. It can be used to synthesis 1-(Phenylsulfonyl)-5-methoxy-1H-indole.

Preparation

The synthesis of 5-methoxyindole from 5-methoxy-2-oxindole: Conversion of 5-methoxy-2-oxindole to 5-methoxyindole was accomplishedby the chlorination of 5-methoxy-2-oxindole with triphenylphosphine-carbontetrachloride in acetonitrile followed by the catalytic reduction of a chlorine atom in 66% total yield.

Definition

ChEBI: 5-methoxyindole is a member of indoles.

Reactions

5-methoxyindole was treated with sodium hydroxide and phenylsulfonyl chloride in the presence of a catalytic amount of tetrabutylammonium bromide to afford 1-(phenylsulfonyl)indole and 5-methoxy-1-(phenylsufonyl)indole in excellent yields of 100%.

Synthesis Reference(s)

Journal of Heterocyclic Chemistry, 26, p. 1405, 1989 DOI: 10.1002/jhet.5570260533
The Journal of Organic Chemistry, 58, p. 5558, 1993 DOI: 10.1021/jo00072a052
Tetrahedron Letters, 27, p. 837, 1986 DOI: 10.1016/S0040-4039(00)84114-3

Purification Methods

Crystallise 5-methoxyindole from cyclohexane pet ether or pet ether/Et2O. [Saito & Kikugawa J Heterocycl Chem 16 1325 1979, Beilstein 21 III/IV 765, 21/3 V 18.]

5-Methoxyindole synthesis

Synthesis of 5-Methoxyindole from 1-Propanone, 1-(5-methoxy-1H-indol-1-yl)-2,2-dimethyl-

5-Methoxyindole Preparation Products And Raw materials

Raw materials

EthenaMine, 2-(5-Methoxy-2-nitrophenyl)-N,N-diMethyl-, (1E)- 1-Propanone, 1-(5-methoxy-1H-indol-1-yl)-2,2-dimethyl- Benzene, 2-ethenyl-4-methoxy-1-nitro- 5-Methoxyindole-3-carboxaldehyde Phosphonium, [2-(1,1-dimethylethoxy)-2-oxoethyl]triphenyl-, inner salt

1-BOC-5-METHOXYINDOLE 5-methoxy-1-[(4-methylphenyl)sulfonyl]-1H-Indole 5-Methoxy-2-nitrobenzaldehyde 5-Methoxy-2,3-dihydroindoline TRIETHANOLAMINE HYDROCHLORIDE

(5-METHOXY-2-NITRO-PHENYL)-ACETONITRILE 5-Methoxy-3-indolecarboxylic acid 5-METHOXYINDOLE-2-CARBOXYLIC ACID 5-Bromoindole

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Preparation Products

5-METHOXY-DL-TRYPTOPHAN 5-METHOXYGRAMINE 2-Amino-5-methoxybenzoic acid

5-Methoxyindole Suppliers

Global( 564)Suppliers

Supplier	Tel	Email	Country	ProdList	Advantage
shanxi leefu-bio technology co. ltd	+86-13021463449 +86-8613021463449	postmaster@leefubio.com	China	153	58
Capot Chemical Co.,Ltd.	571-85586718 +8613336195806	sales@capotchem.com	China	29811	60
Henan Tianfu Chemical Co.,Ltd.	+86-0371-55170693 +86-19937530512	info@tianfuchem.com	China	21975	55
ATK CHEMICAL COMPANY LIMITED	+undefined-21-51877795	ivan@atkchemical.com	China	31969	60
career henan chemical co	+86-0371-86658258	sales@coreychem.com	China	29922	58
Zhejiang ZETian Fine Chemicals Co. LTD	18957127338	stella@zetchem.com	China	2141	58
Hubei Jusheng Technology Co.,Ltd.	18871490254	linda@hubeijusheng.com	CHINA	28184	58
Hebei Guanlang Biotechnology Co., Ltd.	+86-19930503282	alice@crovellbio.com	China	8877	58
Changzhou Ditong Chemical Co.,Ltd	+86-0519-88299272	info@edengenechem.com	China	2169	58
Shandong chuangyingchemical Co., Ltd.	18853181302	sale@chuangyingchem.com	CHINA	5911	58

Supplier	Advantage
shanxi leefu-bio technology co. ltd	58
Capot Chemical Co.,Ltd.	60
Henan Tianfu Chemical Co.,Ltd.	55
ATK CHEMICAL COMPANY LIMITED	60
career henan chemical co	58
Zhejiang ZETian Fine Chemicals Co. LTD	58
Hubei Jusheng Technology Co.,Ltd.	58
Hebei Guanlang Biotechnology Co., Ltd.	58
Changzhou Ditong Chemical Co.,Ltd	58
Shandong chuangyingchemical Co., Ltd.	58

View Lastest Price from 5-Methoxyindole manufacturers

Update time	Product	Price	Min. Order	Purity	Supply Ability	Manufacturer
2023-07-25	5-Methoxyindole 1006-94-6	US $20.00-10.00 / kg	1kg	99%	2T	Hebei Yanxi Chemical Co., Ltd.
2023-05-10	5-Methoxyindole 1006-94-6	US $10.00 / kg	1kg	99%	5000kg	shanxi leefu-bio technology co. ltd
2023-05-09	5-Methoxyindole 1006-94-6	US $10.00 / kg	1kg	99%	5000kg	shanxi leefu-bio technology co. ltd

5-Methoxyindole
1006-94-6
US $20.00-10.00 / kg
99%
Hebei Yanxi Chemical Co., Ltd.

5-Methoxyindole
1006-94-6
US $10.00 / kg
99%
shanxi leefu-bio technology co. ltd

5-Methoxyindole
1006-94-6
US $10.00 / kg
99%
shanxi leefu-bio technology co. ltd

5-Methoxyindole Spectrum

5-Methoxyindole(1006-94-6)MS 5-Methoxyindole(1006-94-6)¹HNMR 5-Methoxyindole(1006-94-6)¹³CNMR 5-Methoxyindole(1006-94-6)IR1 5-Methoxyindole(1006-94-6)IR2 5-Methoxyindole(1006-94-6)IR3 5-Methoxyindole(1006-94-6)Raman

1006-94-6(5-Methoxyindole)Related Search:

Kresoxim-methyl METSULFURON METHYL 3-Methoxybenzaldehyde 5-Methylindole 5-Methoxy-3-indolecarboxylic acid

4-METHOXYINDOLE 98+% (Trifluoromethoxy)benzene 5-Bromoindole 7-Methoxy-1H-indole Tribenuron methyl

Methyl 4'-Methoxyacetophenone p-Anisidine Thiophanate-methyl Parathion-methyl

Methyl salicylate 5-METHOXYINDOLE-2-CARBOXYLIC ACID ABOUT 97% 6-METHOXYINDOLE 99%

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Methoxyindole 99% indol-5-yl methyl ether 5-Methoxyindole ,98% 5-METHOXYINDOLE (5MeOI) 5-methoxy-1H-indole(SALTDATA: FREE) 5-MethoxyindoleF 5-METHOXYINDOLE REPANIDAL NSC 521752 5-METHOXYINDOLE AKOS JY2082918 5-METHOXY-1H-INDOLE RARECHEM AH BS 0117 5-Methoxyindole in stock Factory TIMTEC-BB SBB004094 1H-Indol-5-yl methyl ether 5-methoxy-indol Femedol Indole, 5-methoxy- Methoxy-5 indole methoxy-5indole 5-Methyoxy Indole 5-methyloxyl indole 5-Methoxylindole Methoxyindole,99% Indol-5-yl methyl ether 5-Methoxyindole> 5-Methoxyindole 1006-94-6 1006-94-6 Indoles Simple Indoles Building Blocks Heterocyclic Building Blocks blocks IndolesOxindoles Heterocycles Indoles and derivatives IndoleDerivative Pyrroles & Indoles Heterocyclic Compounds Indole Series Indoles Indoline & Oxindole Indole Building Blocks C7 to C9 Chemical Synthesis Heterocyclic Building Blocks Heterocycle-Indole series Indole Derivatives Simple Indoles Chiral Compound Pyrroles & Indoles Building Blocks Heterocyclic Building Blocks